Artigos Científicos - FAGEO/IG
URI Permanente para esta coleçãohttps://repositorio.ufpa.br/handle/2011/2801
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Navegando Artigos Científicos - FAGEO/IG por Autor "ANGÉLICA, Rômulo Simões"
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Item Acesso aberto (Open Access) Application of bauxite waste from amazon region in the heavy clay industry(2013-12) HILDEBRANDO, Edemarino Araujo; SOUZA, José Antônio da Silva; ANGÉLICA, Rômulo Simões; NEVES, Roberto de FreitasIn this work, a method was developed for the application of red mud, an alkaline leaching waste, from a bauxite processing plant located in northern Brazil (Amazon region) as starting material for heavy clay products. Samples were prepared by pressing blends of red mud and clay, which were then fired at temperatures from 900 ºC to 1190 ºC. Characterization was carried out by chemical analysis, differential thermal analysis (DTA) and X-ray diffraction (XRD), and the following ceramic properties were evaluated: water absorption, linear shrinkage and flexural strength. In order to evaluate the Na+ stability in the dense ceramic, leaching tests were also carried out on the specimens after sintering process. Results indicated that samples with 50 and 70 wt% of red mud are proper for being used in the production of ceramic bodies, due to its excellent properties, mainly high mechanical resistance and low water absorption, showing thus, an option to minimizing the environmental impacts caused by the aluminum industry.Item Acesso aberto (Open Access) Avaliação tecnológica de cerâmicas tradicionais incorporadas com rejeito do minério de manganês(2014-12) RODRIGUES, L. dos S.; SILVA, J. C.; ANGÉLICA, Rômulo Simões; RABELO, A. A.; FAGURY, Renata Lilian Ribeiro Portugal; FAGURY NETO, EliasThe ceramic industry has a great environmental role when it comes to recycling waste. The industrial production that has been developed in the Northern Region of Brazil makes room for use of waste as a substitute raw material in the production of ceramics. This substitution in addition to the environmental advantage also provides interesting physical characteristics in the ceramics produced. This work aimed to study the effects caused by the incorporation of manganese ore tailings in formulations of ceramic clay, to examine the extent to which it is possible to incorporate this waste without prejudice to the product properties. It was proposed some formulations containing varying amounts of tailings. The ceramic bodies were shaped and sintered at 1000 ºC to 1200ºC for 2 h. Results demonstrated that the material showed a decreasing in the porosity and water absorption, and an increasing in the bending strength as a result of the densification promoted by the tailing incorporation which acts as fluxing agent.Item Acesso aberto (Open Access) Synthesis and characterization of zeolite NaP using kaolin waste as a source of silicon and aluminum(2014-08) HILDEBRANDO, Edemarino Araujo; ANDRADE, Christiano Gianesi Bastos; ROCHA JUNIOR, Carlos Augusto Ferreira da; ANGÉLICA, Rômulo Simões; DIAZ, Francisco Rolando ValenzuelaThe synthesis of zeolite NaP using kaolin waste, from the Amazon region, as a predominant source of silicon and aluminum has been studied. The zeolitisation process occurred in hydrothermal conditions using static autoclaving and the effects of time, temperature, and the Si/Al ratio were investigated. The starting material and the phases formed as reaction products were characterized by XRD, SEM and FTIR. The results showed that pure zeolite NaP is hydrothermally synthesized, at 100 °C for 20 hours, using metakaolin waste material in alkaline medium in presence of additional silica. The XRD and SEM analyses indicate that the synthesized zeolite presents good crystallinity.