Navegando por Autor "PENA, Rosinelson da Silva"

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Acesso aberto (Open Access)
Adsorption capacity of phenolic compounds onto cellulose and xylan
(Universidade Federal do Pará, 2015-06) COSTA, Telma dos Santos; ROGEZ, Hervé Louis Ghislain; PENA, Rosinelson da Silva
The interaction between three phenolic compounds (catechin, caffeic acid and ferulic acid) onto two dietary fibres (cellulose and xylan) has been evaluated to inquire possible interferences on the biodisponibility of phenolic compounds. The adsorption kinetics were performed using solutions containing 100 mg/L of phenolic compounds during a contact time ranging between 10 and 120 minutes at pH 2.0, 4.5, and 7.0. After the kinetics, isotherms were obtained using phenolic compounds concentration ranging between 10 and 80 mg/L during 60 minutes, at pH 2.0 and 7.0 and temperature of 36 °C. Results indicate that adsorbed quantities mainly changed in function of pH, however the maximum adsorption was only of 0.978 mg of caffeic acid/g of xylan at pH 2 and after 60 min. Redlich-Peterson model were able to predict the adsorption isotherms of all phenolic compounds onto cellulose, except for caffeic acid at pH 7.0. The low adsorption capacities observed suggest that both dietary fibres are unable to compromise the biodisponibility of phenolic compounds, especially in the small intestine, where they are partially absorbed.
Acesso aberto (Open Access)
Aplicação de modelos matemáticos bi e tri-paramétricos na predição de isotermas de adsorção de umidade do guaraná (Paullinia cupana) em pó
(2000-04) PENA, Rosinelson da Silva; RIBEIRO, Claudio Cavalcanti; GRANDI, José Glauco
In this study, twelve mathematic models (six biparametrics and six triparametrics), applied in the prediction of isotherms, were studied on prediction of moisture adsorption isoterms of guarana (Paullinia cupana) powder obtained in spray dryer. The moisture adsorption isotherms of the product were fitted at 15° C, 25° C and 35° C, by nonlinear regression analysis, using the software STATGRAPHICS 5.1. The best results among studied models on prediction of moisture adsorption isotherms were GAB, modified BET and Anderson equations (triparametric), Handerson and Oswin equations (biparametric).
Acesso aberto (Open Access)
Caracterização de farinhas de tapioca produzidas no estado do Pará
(2013) SILVA, Priscilla Andrade; CUNHA, Roberto Lisboa; LOPES, Alessandra Santos; PENA, Rosinelson da Silva
Tapioca flour is a typical food produced from cassava starch (Manihot esculenta Crantz), widely consumed in the Amazon Region. The aim of this study was to characterize two tapioca flours produced in Pará State, Brazil one in the West Region and other in Bragantina Area. Both tapioca flour presented distinct particle-size distribution and significant difference (P0.05) for majority of the physico-chemical and technological parameters. Flour from West Region presented high moisture (10.7%), this due the greater capacity of water adsorption, attributed at its high specific area (smaller particlesize). The optical microscopy with polarized light and the technologic properties of the products did not showed a standard process for the production of tapioca flour.
Acesso aberto (Open Access)
Caracterização e processamento de leite bubalino em pó em secador por nebulização
(2005-09) GUERRA, Roberta Batista; NEVES, Elisa Cristina Andrade; PENA, Rosinelson da Silva
This work aims to show the process development based on the spray dryer for the obtaining of powdered buffalo milk. For that, physiochemical analyses were made in the milk in natura and later in the powdered product, which was also submitted to microbiological analysis to be sure that it could be consumed by humans; and to sensorial analysis for obtaining information about the product's acceptance. Sorption isotherms for the powdered product were obtained at 25ºC with the purpose of perceiving the hygroscopic behavior. The buffalo's powdered milk presented the following characteristics: 3,4 % moisture content, 23,2% proteins, 46,1% fat, 4,2% ash, 0,5% soybean lecithin and 22,6% of total carbohydrates. The product was characterized as whole powdered buffalo milk, because it didn't suffer any standardization. Nutrient losses, during the process, were less then 5%, and just for proteins the variation was more than 15%. It can be justified by the desnaturation of the casein due to high temperatures (>80ºC). The powdered product presented type III sorption isotherms and the same behavior was observed for the whole powdered milk. Through sorption isotherms, the moisture content value, referent to the monolayer, was on an average of 4,4g H2O/100g dry solids, which confirms the process efficiency. The hysteresis behavior presented by the powdered product was similar of the whole powdered milk. The product acceptance was of 74%, close to the commercial powdered milk acceptance.
Acesso aberto (Open Access)
Chemical composition of different muscle zones in pirarucu (Arapaima gigas)
(Universidade Federal do Pará, 2017-04) MARTINS, Mayara Galvão; MARTINS, Déborah Elena Galvão; PENA, Rosinelson da Silva
Identifying potential patterns in pirarucu (Arapaima gigas) composition, as a function of the different fish muscle zones (dorse, venter, ventrecha and tail), was the main objective of this research. For such, the different pirarucu muscle zones were evaluated, in order to obtain proximate composition and minerals content. It was also determined amino acids and fatty acids contents in fish muscle. The dorsal, ventral and tail muscle zones presented similar moisture (76.5-78.2%), protein (17.8-18.9%), total lipids (1.0-1.5%) and ash (0.9-1.2%) contents. On the other hand, the ventrecha zone presented 25.8% of protein and the major total lipids content (17.1%). The main minerals found in fish muscle were K (183.5-288.6 mg/100 g muscle) and Na (65.1-175.5 mg/100 g). Glutamic acid (3027.6 mg/100 g muscle) was the main amino acid found in fish muscle, which presented 48% of essential amino acids in the protein fraction. Lipids content showed 57.3% of unsaturated fatty acids and 42.7% of saturated fatty acids.
Acesso aberto (Open Access)
Comportamento higroscópico da farinha de pupunha (Bactris gasipaes)
(2003-08) FERREIRA, Cristiane Damasceno; PENA, Rosinelson da Silva
It was studied the hygroscopic behavior of the pupunha flour obtained by drying in the oven at 70°C. It was collected data of moisture adsorption for two temperatures (15°C and 35°C), using the static method, where the recipients with the capacity of 500mL, having saturated salt solutions, it was used as environment generators of constant relative humidity, ranging from 11% to 97%, which were submitted the samples of the product. From the equilibrium data, it was built isotherms of moisture adsorption, being observed type III isotherms, but even that the equilibrium moisture for the product decreases with the temperature increase. It was determined the isosteric heat of adsorption for different levels of equilibrium moisture and the equivalent moisture to the monolayer, which were inferior of 5g H2O/100 g s.s. It was verified the application of the GAB model in the equilibrium data prediction for the product. According to the results obtained, the pupunha flour shows low hygroscopicity, low affinity for water molecule.
Acesso aberto (Open Access)
Comportamento higroscópico do açaí e cupuaçu em pó
(2008-12) SILVA, Alessandra Eluan da; SILVA, Luiza Helena Meller da; PENA, Rosinelson da Silva
The aim of this work was to evaluate experimentally the adsorption and desorption isotherm of açaí (Euterpe oleracea) and cupuaçu (Theobroma grandiflorum) powders using a hygrometer AQUAlab3TE of Decagon. Three levels of temperature (15, 25 and 35 °C) were tested. The type III curves obtained suggest the materials are rich in carbohydrates. Four mathematical models were fitted to the experimental data, Handerson, Oswin, GAB, and modified BET by nonlinear regression analysis using the software STATISTICA for Windows 5.1B. The Oswin and GAB models were better fitted to the açaí and cupuaçu powder sorption data, respectively. The monolayer for açaí and cupuaçu powders was determined. The desorption heat of the açaí powder was also determined.
Acesso aberto (Open Access)
Comportamento higroscópico do resíduo seco de camarão-rosa
(2007-12) ASSUNÇÃO, Alan Barros; PENA, Rosinelson da Silva
A study was made of the hygroscopic behavior of the dry residue of pink shrimp (Peneaus subtilis), characterized as being rich in total proteins (42.59%) and ash (22.01%). Adsorption and desorption isotherms were plotted at 10, 25 and 40 °C. The monolayer and desorption heat values were determined and thirteen mathematical models were fitted to experimental data to predict the sorption data. The product presented Type II isotherms. The adsorption data indicated that the product's microbiological stability (aw < 0.6) would require the dry residue to contain moisture of less than 13.0 g H2O.100 g–1 dry solids in adsorption and 14.0 g H2O.100 g–1 dry solids in desorption. The monolayer's desorption values indicated that, in order to avoid unnecessary loss of energy, the residue should not be dried to a moisture level below 7.29 g H2O.100 g–1 dry solids. The values of desorption heat indicated that large amounts of energy were not required to dry the residue to appropriate levels of moisture to attain microbiological stability (aw < 0.6). The best models for predicting the sorption isotherms of the residue were Oswin and Halsey (biparametric); GAB, modified BET, Hailwood-Horrobin, Anderson, Anderson-Hall and Gascoyne-Pethig (triparametric).
Acesso aberto (Open Access)
Hygroscopic behavior of buriti (Mauritia flexuosa) fruit
(2011-12) MELO, Wellington dos Santos; PENA, Rosinelson da Silva; RODRIGUES, Antonio Manoel da Cruz; SILVA, Luiza Helena Meller da
The objective of this study was to perform an analysis of the characterization of buriti fruit (Mauritia flexuosa). Each part of the fruit (peel, pulp, and fibrous part) was analyzed and their hygroscopic behavior was evaluated to establish the drying and storage conditions. Adsorption and desorption isotherms were obtained at 25 °C to the monolayer value was estimated, and the application of the Halsey, Handerson, Kuhn, Mizrahi, Oswin, Smith, BET, and GAB models was evaluated to the prediction of the isotherms. The fruit pulp was classified as rich in high quality oil, and like the peel and the fibrous part, it was also considered as rich in dietary fiber. The isotherms of the fruit parts were classified as type II, and their microbiological stability (aw< 0.6) can be maintained at 25 °C if the moisture content is lower than 8.5, 7.3, and 11.0 g H2O.100 g-1 of dry matter (d.m.), respectively. The hygroscopic behavior showed that in order to ensure stability, the fruit parts should be packaged with low water vapor permeability. The monolayer demonstrated that the peel, pulp, and the fibrous part cannot be dried under moisture content lower than 5.9, 5.0, and 6.4 g H2O.100 g-1 d.m., respectively. GAB was the most adequate model to describe their isotherms.
Acesso aberto (Open Access)
Hygroscopic behaviour of cassava flour from dry and water groups
(Universidade Federal do Pará, 2015-08) CHISTÉ, Renan Campos; CARDOSO, Jonnahta Monteiro; SILVA, Diego Aires da; PENA, Rosinelson da Silva
Cassava flour from dry and water groups are important starch products widely consumed in the Amazonian region of Brazil. In this study, the moisture sorption isotherms of cassava flour from dry and water groups were obtained in the water activity (aw) range from 0.09 to 0.94 (dry group) and 0.07 to 0.93 (water group) at 25°C and the applicability of eight mathematical models in data prediction was evaluated. Both cassava flour from dry and water groups exhibited type II isotherms (sigmoid) and the hysteresis effect between adsorption and desorption isotherms was shown almost over the entire range of aw. The moisture of cassava flour from dry and water groups should not exceed 11.3g H2O 100g-1(aw=0.6) to ensure the theoretical microbiological stability and the monolayer moisture value (9.0 and 7.9 g H2O 100g-1, respectively) indicated the level of moisture content to be reached during the drying process to avoid unnecessary power consumption. Finally, the data fit showed that the mathematical model of GAB were able to predict efficiently the sorption isotherms of both cassava flour from dry and water group at the entire aw range.
Acesso aberto (Open Access)
Influência da temperatura nos parâmetros de modelos bi-paramétricos que predizem isotermas de adsorção de umidade do guaraná (Paullinia cupana) em pó
(1997-12) PENA, Rosinelson da Silva; RIBEIRO, Claudio Cavalcanti; GRANDI, José Glauco
Eight biparametric mathematic models of the literature and widely applied in the prediction of moisture adsorption isoterms were analised. The guarana (Paullinia cupana) powder used in this study, was obtained in spray dryer from a hidroalcoholic extract. The experimental points of the moisture adsorption isotherms of the product at 15°C, 25°C and 35°C were fitted by non-linear regression analysis. To study temperature effect in the parameters of the models were used linear, exponential, logarithmic and inverse regressions. They were also used to fit the software STATGRAPHICS 5.1. The Handerson, Oswin and Mizrahi equations presented the best results among tested models.
Acesso aberto (Open Access)
Physicochemical properties of three sugary cassava landraces
(2013-05) SOUZA, Hugo Antonio Lima de; BENTES, Ádria de Sousa; LADEIRA, Taiana Marina Souza; LOPES, Alessandra Santos; PENA, Rosinelson da Silva
This study evaluates the physical and physicochemical properties of three sugary cassava (Manihot esculenta Crantz) landraces: São Francisco Bag 3, Manicueira 62, and Castanhal Iracema. These three landraces showed high estimated productivity (≥3.93kg plant-1) and had a high sugar content (≥3.92g 100g-1 of root), making them viable for use in syrup production, especially the São Francisco Bag 3 landrace (4.76g 100g-1). The Manicueira 62 landrace had the highest starch content (4.40g 100g-1). The three sugary cassava landraces exhibited high levels of cyanide (>195mg kg-1), indicating the need for processing prior to consumption.
Acesso aberto (Open Access)
Production of medium-chain-length polyhydroxyalkanoate by Pseudomonas oleovorans grown in sugary cassava extract supplemented with andiroba oil
(2014-12) SILVA, Diego Aires da; ANTONIO, Regina Vasconcellos; ROSSI, José Márcio; PENA, Rosinelson da Silva
Pseudomonas oleovorans were grown on sugary cassava extracts supplemented with andiroba oil for the synthesis of a mediumchain- length polyhydroxyalkanoate (PHAMCL). The concentration of total sugars in the extract was approximately: 40 g/L in culture 1, 15 g/L in cultures 2 and 3, and 10 g/L in culture 4. Supplementation with 1% andiroba oil and 0.2 g/L of (NH4)2HPO4 was performed 6.5 hours after growth in culture 3, and supplementation with the same amount of andiroba oil and 2.4 g/L of (NH4)2HPO4 was performed at the beginning of growth in culture 4. The synthesis resulted mainly in 3-hydroxy-decanoate and 3-hydroxy-dodecanoate units; 3-hydroxy-butyrate, 3-hydroxy-hexanoate; and 3-hydroxy-octanoate monomers were also produced but in smaller proportions. P. oleovorans significantly accumulated PHAMCL in the deceleration phase of growth with an oxygen limitation but with sufficient nitrogen concentration to maintain cell growth. The sugary cassava extract supplemented with andiroba oil proved to be a potential substrate for PHAMCL production.
Acesso aberto (Open Access)
Qualidade física e sensorial de biscoitos doces com fécula de mandioca
(2010-12) VIEIRA, Jucyanne Carvalho; MONTENEGRO, Flávio Martins; LOPES, Alessandra Santos; PENA, Rosinelson da Silva
This research evaluated the substitution of 5, 10 and 15% of wheat flour for cassava starch in sweet cookies production. Both, flour and starch were submitted to the physicochemical, rheological and differential thermal analysis (DTA). The produced cookies were compared through sensory and microbiological analyses. The DTA result didn´t show any alteration in the starch gelatinization behavior. The result of the sensory acceptance analysis showed that crispness is the unique attribute that presented significant difference, indicating the technical viability of wheat flour substitution for 15% of cassava starch.
Acesso aberto (Open Access)
Rheological behavior of Brazilian Cherry (Eugenia uniflora L.) pulp at pasteurization temperatures
(2013-03) LOPES, Alessandra Santos; MATTIETTO, Rafaella de Andrade; MENEZES, Hilary Castle de; SILVA, Luiza Helena Meller da; PENA, Rosinelson da Silva
The rheological behavior of Brazilian Cherry (Eugenia uniflora L.) pulp in the range of temperatures used for pasteurization (83 to 97 °C) was studied. The results indicated that Brazilian Cherry pulp presented pseudoplastic behavior, and the Herschel-Bulkley model was considered more adequate to represent the rheological behavior of this pulp in the range of temperatures studied. The fluid behavior index (n) varied in the range from 0.448 to 0.627. The effect of temperature on the apparent viscosity was described by an equation analogous to Arrhenius equation, and a decrease in apparent viscosity with an increase in temperature was observed.
Acesso aberto (Open Access)
Rheological behavior of concentrated tucupi
(Universidade Federal do Pará, 2018-11) COSTA, Telma dos Santos; RODRIGUES, Antonio Manoel da Cruz; PENA, Rosinelson da Silva
Tucupi, which is widely enjoyed in the North region of Brazil, is a fermented liquid derived from cassava (Manihot esculenta Crantz) and has been taken abroad for its exotic characteristics. This study aimed to assess the rheological behavior of tucupi with 30, 35, and 40% solids and concentrated at 50, 70, and 90 °C. The rheological data were obtained at 25, 40, 60, and 80 °C with increasing and decreasing shear rates. Rheology at 25 °C indicated that the partial gelification of starch during concentration causes a decrease in the product’s viscosity and, if the concentration is carried out at a temperature that favors total starch gelification, the product’s viscosity increases. Concentrated tucupi behaved as a pseudoplastic fluid, but at 60 and 80 °C with increasing shear rates, the product behaved as a dilatant fluid. Hysteresis were observed in flow curves starting at 40 °C, which characterizes concentrated tucupi as a rheopectic fluid. The Ostwald-de Waele model predicted the product’s flow curves and an Arrhenius-like equation described the dependence of temperature on apparent viscosity for the rheological data obtained with increasing shear rates. The product’s activation energy (E a) values ranged from 16.86 to 25.23 kJ/mol as a function of concentration.